Manipulation of nanoparticles of different shapes inside a scanning electron microscope

Beilstein J Nanotechnol. 2014 Feb 5:5:133-40. doi: 10.3762/bjnano.5.13. eCollection 2014.

Abstract

In this work polyhedron-like gold and sphere-like silver nanoparticles (NPs) were manipulated on an oxidized Si substrate to study the dependence of the static friction and the contact area on the particle geometry. Measurements were performed inside a scanning electron microscope (SEM) that was equipped with a high-precision XYZ-nanomanipulator. To register the occurring forces a quartz tuning fork (QTF) with a glued sharp probe was used. Contact areas and static friction forces were calculated by using different models and compared with the experimentally measured force. The effect of NP morphology on the nanoscale friction is discussed.

Keywords: contact mechanics; nanomanipulation; nanoparticles; nanotribology; scanning electron microscopy (SEM).