Influence of radiopaque fillers on physicochemical properties of a model epoxy resin-based root canal sealer

J Appl Oral Sci. 2013 Nov-Dec;21(6):533-9. doi: 10.1590/1679-775720130334.

Abstract

Objective: To verify the influence of radiopaque fillers on an epoxy resin-based sealer.

Material and methods: Experimental sealers were formulated by adding 20%, 40%, 60%, 80%, 100% and 120% of calcium tungstate, ytterbium trifluoride or barium sulphate by weight to an epoxy-resin-base. Setting time, flow, film thickness, radiopacity, sorption, solubility, pH and push-out bond strength were evaluated.

Results: The setting time ranged from 373 to 612.66 min, the flow varied from 13.81±0.49 to 22.49±0.37 mm, and the film thickness ranged from 16.67±5.77 to 33.33±11.54 µm. The lowest pH was 5.47±0.53, and the highest was 6.99±0.03. Radiopacity varied from 0.38±0.04 to 2.57±0.21 mmAl and increased with the amount of filler. Calcium tungstate sealers had a higher sorption and solubility than other sealers. There was no significant difference in the push-out bond strength among the fillers at the 120% concentration.

Conclusion: The inorganic fillers evaluated and their concentrations affect the physicochemical properties of an epoxy resin-based root canal sealer.

Publication types

  • Evaluation Study

MeSH terms

  • Analysis of Variance
  • Barium Sulfate / chemistry
  • Calcium Compounds / chemistry
  • Contrast Media / chemistry
  • Dental Bonding / methods*
  • Epoxy Resins / chemistry*
  • Materials Testing
  • Particle Size
  • Reference Values
  • Reproducibility of Results
  • Root Canal Filling Materials / chemistry*
  • Solubility
  • Statistics, Nonparametric
  • Surface Properties
  • Tungsten Compounds / chemistry
  • Ytterbium / chemistry

Substances

  • Calcium Compounds
  • Contrast Media
  • Epoxy Resins
  • Root Canal Filling Materials
  • Tungsten Compounds
  • epoxy resin-based root canal sealer
  • Barium Sulfate
  • calcium tungstate
  • Ytterbium