4-Meth-oxy-N-[(4-methyl-phen-yl)sulfon-yl]benzamide including an unknown solvate

Swamy Sreenivasa; Bandrehalli Siddagangaiah Palakshamurthy; Jagdish Tonannavar; Yenagi Jayashree; Achar Gurumurthy Sudha; Parameshwar Adimoole Suchetan

doi:10.1107/S1600536813028158

4-Meth-oxy-N-[(4-methyl-phen-yl)sulfon-yl]benzamide including an unknown solvate

Acta Crystallogr Sect E Struct Rep Online. 2013 Oct 19;69(Pt 11):o1664-5. doi: 10.1107/S1600536813028158.

Authors

Swamy Sreenivasa¹, Bandrehalli Siddagangaiah Palakshamurthy², Jagdish Tonannavar³, Yenagi Jayashree³, Achar Gurumurthy Sudha⁴, Parameshwar Adimoole Suchetan⁵

Affiliations

¹ Department of Studies and Research in Chemistry, Tumkur University, Tumkur, Karnataka 572 103, India.
² Department of Studies and Research in Physics, U.C.S., Tumkur University, Tumkur, Karnataka 572 103, India.
³ Department of Physics, Karnatak University, Dharwad, Karnataka 580 003, India.
⁴ University College of Science, Tumkur University, Tumkur, India.
⁵ Department of Studies and Research in Chemistry, U.C.S., Tumkur University, Tumkur, Karnataka 572 103, India.

Abstract

In the title compound, C15H15NO4S, the dihedral angle between the benzene rings is 78.62 (16)°. In the crystal, adjacent mol-ecules are linked along the c axis into C(4) chains through strong N-H⋯O hydrogen bonds. Mol-ecules are further connected through C-H⋯O hydrogen bonds into a hexa-meric unit generating an R (6) 6(66) motif. Another C-H⋯O inter-action connects the mol-ecules along the c axis, forming C(5) chains. A region of disordered electron density, most probably disordered methanol-water solvent mol-ecules, was treated with the SQUEEZE routine in PLATON [Spek (2009 ▶). Acta Cryst. D65, 148-155]. The formula mass and unit-cell characteristics do not take into account this disordered solvent.