NMR methodology for complex mixture 'separation'

Nicholle G A Bell; Lorna Murray; Margaret C Graham; Dušan Uhrín

doi:10.1039/c3cc48907h

NMR methodology for complex mixture 'separation'

Chem Commun (Camb). 2014 Feb 18;50(14):1694-7. doi: 10.1039/c3cc48907h.

Authors

Nicholle G A Bell¹, Lorna Murray, Margaret C Graham, Dušan Uhrín

Affiliation

¹ EastChem, School of Chemistry, University of Edinburgh, King's Buildings, West Mains Rd, Edinburgh, Scotland EH9 3JJ, UK. dusan.uhrin@ed.ac.uk.

PMID: 24395014
DOI: 10.1039/c3cc48907h

Abstract

Mixture 'separation' by NMR is demonstrated through the development of a pseudo 4D NMR experiment, 3D IPAP INEPT-INADEQUATE-HSQC, designed for the structural elucidation of (13)C tagged compounds.