Bond strength of different resin cement and ceramic shades bonded to dentin

J Adhes Dent. 2013 Oct;15(5):461-6. doi: 10.3290/j.jad.a29591.

Abstract

Purpose: To evaluate the microtensile bond strength (MTBS) of ceramic cemented to dentin varying the resin cement and ceramic shades.

Materials and methods: Two VITA VM7 ceramic shades (Base Dentine 0M1 and Base Dentine 5M3) were used. A spectrophotometer was used to determine the percentage translucency of ceramic (thickness: 2.5 mm). For the MTBS test, 80 molar dentin surfaces were etched and an adhesive was applied. Forty blocks (7.2 x 7.2 x 2.5 mm) of each ceramic shade were produced and the ceramic surface was etched (10% hydrofluoric acid) for 60 s, followed by the application of silane and resin cement (A3 yellow and transparent). The blocks were cemented to dentin using either A3 or transparent cement. Specimens were photoactivated for 20 s or 40 s, stored in distilled water (37°C/24 h), and sectioned. Eight experimental groups were obtained (n = 10). Specimens were tested for MTSB using a universal testing machine. Data were statistically analyzed using ANOVA and Tukey's post-hoc tests (α <= 0.05).

Results: The percentage translucency of 0M1 and 5M3 ceramics were 10.06 (± 0.25)% and 1.34 (± 0.02)%, respectively. The lowest MTBS was observed for the ceramic shade 5M3. For the 0M1 ceramic, the A3 yellow cement that was photocured for 20 s exhibited the lowest MTBS, while the transparent cement that was photocured for 40 s presented the highest MTBS.

Conclusions: For the 2.5-mm-thick 5M3 ceramic restorations, the MTBS of ceramic cemented to dentin significantly increased. The dual-curing cement Variolink II photocured for 40 s is not recommended for cementing the Base Dentine 5M3 feldspathic ceramic to dentin.

Publication types

  • Comparative Study
  • Randomized Controlled Trial

MeSH terms

  • Acid Etching, Dental / methods
  • Aluminum Silicates / chemistry
  • Cementation / methods
  • Ceramics / chemistry
  • Color
  • Dental Bonding*
  • Dental Cements / chemistry
  • Dental Porcelain / chemistry*
  • Dental Stress Analysis / instrumentation
  • Dentin / anatomy & histology*
  • Humans
  • Hydrofluoric Acid / chemistry
  • Light-Curing of Dental Adhesives
  • Materials Testing
  • Methacrylates / chemistry
  • Microscopy, Electron, Scanning
  • Phosphoric Acids / chemistry
  • Potassium Compounds / chemistry
  • Resin Cements / chemistry*
  • Silanes / chemistry
  • Spectrophotometry
  • Stress, Mechanical
  • Surface Properties
  • Temperature
  • Tensile Strength
  • Time Factors
  • Water / chemistry

Substances

  • Aluminum Silicates
  • Dental Cements
  • Excite cement
  • Methacrylates
  • Monobond S
  • Phosphoric Acids
  • Potassium Compounds
  • Resin Cements
  • Silanes
  • VITA VM7
  • Water
  • Dental Porcelain
  • feldspar
  • Variolink
  • phosphoric acid
  • Hydrofluoric Acid