Degree of conversion of polymer-matrix composite assessed by FTIR analysis

J Contemp Dent Pract. 2013 Jan 1;14(1):76-9. doi: 10.5005/jp-journals-10024-1274.

Abstract

Aims and objectives: The behavior of polymer-matrix composite is dependent on the degree of conversion. The aim of this study was to evaluate the degree of conversion of two resin cements following storage at 37°C immediately, 24 and 48 hours, and 7 days after light-curing by FTIR analysis.

Materials and methods: The specimens were made in a metallic mold and cured with blue LED with power density of 500 mW/ cm(2) for 30 seconds. The specimens were pulverized, pressed with KBr and analyzed with FTIR following storage times.

Statistical analysis used: ANOVA (two-way) and Tukey's post hoc.

Results: To the polymer-matrix composites between 24 and 48 hours does not show a significant increase (p > 0.05), however, the highest values were found after 7 days.

Conclusion: The polymer-matrix composites used in this study showed similarity on the degree of conversion and increased of according to the time of storage.

MeSH terms

  • Bisphenol A-Glycidyl Methacrylate / chemistry
  • Carbon / chemistry
  • Composite Resins / chemistry*
  • Composite Resins / radiation effects
  • Curing Lights, Dental / classification
  • Humans
  • Light-Curing of Dental Adhesives
  • Materials Testing
  • Methacrylates / chemistry
  • Polyethylene Glycols / chemistry
  • Polymerization
  • Polymers / chemistry
  • Polymers / radiation effects
  • Polymethacrylic Acids / chemistry
  • Polyurethanes / chemistry
  • Radiation Dosage
  • Resin Cements / chemistry*
  • Resin Cements / radiation effects
  • Self-Curing of Dental Resins
  • Spectroscopy, Fourier Transform Infrared
  • Temperature
  • Time Factors
  • Tricarboxylic Acids / chemistry

Substances

  • Composite Resins
  • Methacrylates
  • Nexus
  • Polymers
  • Polymethacrylic Acids
  • Polyurethanes
  • Resin Cements
  • Tricarboxylic Acids
  • urethane dimethacrylate luting resin
  • triethylene glycol dimethacrylate
  • Polyethylene Glycols
  • Bisphenol A-Glycidyl Methacrylate
  • 4-methacryloxyethyltrimellitic acid
  • hydroxyethyl methacrylate
  • Carbon