A compact high vacuum heating chamber for in-situ x-ray scattering studies

Rev Sci Instrum. 2012 Aug;83(8):083904. doi: 10.1063/1.4746290.

Abstract

A very compact multi purpose high vacuum heating chamber for x-ray scattering techniques was developed. The compact design allows the chamber to be installed on high precision diffractometers which usually cannot support heavy and/or large equipment. The chamber is covered by a Be dome allowing full access to the hemisphere above the sample which is required for in-plane grazing incident x-ray diffraction and out-off plane wide angle x-ray diffraction.