Characterizations of additive manufactured porous titanium implants

J Biomed Mater Res B Appl Biomater. 2012 Oct;100(7):1970-9. doi: 10.1002/jbm.b.32764. Epub 2012 Aug 2.

Abstract

This article describes physical, chemical, and mechanical characterizations of porous titanium implants made by an additive manufacturing method to gain insight into the correlation of process parameters and final physical properties of implants used in orthopedics. For the manufacturing chain, the powder metallurgy technology was combined with the additive manufacturing to fabricate the porous structure from the pure tanium powder. A 3D printing machine was employed in this study to produce porous bar samples. A number of physical parameters such as titanium powder size, polyvinyl alcohol (PVA) amount, sintering temperature and time were investigated to control the mechanical properties and porosity of the structures. The produced samples were characterized through porosity and shrinkage measurements, mechanical compression test and scanning electron microscopy (SEM). The results showed a level of porosity in the samples in the range of 31-43%, which is within the range of the porosity of the cancelluous bone and approaches the range of the porosity of the cortical bone. The results of the mechanical test showed that the compressive strength is in the wide range of 56-509 MPa implying the effect of the process parameters on the mechanical strengths. This technique of manufacturing of Ti porous structures demonstrated a low level of shrinkage with the shrinkage percentage ranging from 1.5 to 5%.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Bone Substitutes / chemistry*
  • Compressive Strength
  • Materials Testing*
  • Microscopy, Electron, Scanning
  • Polyvinyl Alcohol / metabolism*
  • Porosity
  • Titanium / chemistry*

Substances

  • Bone Substitutes
  • Polyvinyl Alcohol
  • Titanium