The influence of long term water immersion on shear bond strength of amalgam repaired by resin composite and mediated by adhesives or resin modified glass ionomers

J Dent. 2012 Jul;40(7):594-602. doi: 10.1016/j.jdent.2012.04.001. Epub 2012 Apr 12.

Abstract

Objective: To assess the shear bond strength between amalgam and resin composite mediated by either multipurpose adhesive systems or RMGI when subjected to long term immersion in saline.

Methods: Part I: Cylindrical specimens (6 mm × 6 mm) composed of equal parts of sandblasted set amalgam (Oralloy) and composite (Z-100), with a thin layer of either Scotchbond Multipurpose, All Bond 2, Amalgam Bond Plus, High Q Bond Plus or Vitrebond in between were fabricated (n = 100 × 5). Each group was divided into 3 subgroups, immersed in saline at 37 °C for either 48 h, 3 or 6 months, followed by thermocycling (5000; 5/55 °C) and shear bond strength testing (SBS). Part II: Identical specimens were fabricated with intermediary of either Ketac Cem, Fuji Lining LC, Rely X Luting, Fuji Plus or Meron Plus (n = 100 × 5). Immersion periods, followed by thermocycling and SBS testing as in Part I. Two representative specimens from each subgroup were sectioned and inspected under SEM.

Results: The two classes of intermediary agents yielded SBS which differed mainly in the 6 months incubation period. While multipurpose adhesives provided SBS values of ~9-10 MPa RMGI provided higher SBS of ~16 MPa. All Bond 2 and Amalgam Bond Plus exhibited deterioration of SBS during the 6 month period as well as Rely X Luting. Gap sizes between 0.5 and 3 μm exist between all intermediaries and the amalgam; on the other hand all intermediaries exhibit gap-free interfaces between the adhesives/RMGI and the composite.

Conclusions: Vitrebond in particular and RMGIs in general can serve as an excellent coupler of resin composite to amalgam, providing a durable bond.

MeSH terms

  • Composite Resins / chemistry*
  • Dental Amalgam / chemistry*
  • Dental Bonding*
  • Dental Cements / chemistry*
  • Dental Etching / methods
  • Dental Materials / chemistry*
  • Dental Restoration Repair / methods*
  • Glass Ionomer Cements / chemistry
  • Humans
  • Magnesium Oxide / chemistry
  • Materials Testing
  • Methacrylates / chemistry
  • Microscopy, Electron, Scanning
  • Polycarboxylate Cement / chemistry
  • Resin Cements / chemistry
  • Shear Strength
  • Silicon Dioxide / chemistry
  • Sodium Chloride / chemistry
  • Stress, Mechanical
  • Surface Properties
  • Temperature
  • Time Factors
  • Water / chemistry*
  • Zinc Oxide / chemistry
  • Zirconium / chemistry

Substances

  • Amalgambond
  • Composite Resins
  • Dental Cements
  • Dental Materials
  • Glass Ionomer Cements
  • Meron
  • Methacrylates
  • Polycarboxylate Cement
  • Resin Cements
  • Scotchbond Multi-Purpose
  • Vitremer
  • Z100 composite resin
  • Water
  • Vitrabond
  • Fuji glass-ionomer lining cement
  • All-Bond 2
  • Magnesium Oxide
  • Sodium Chloride
  • Silicon Dioxide
  • Dental Amalgam
  • Ketac-cem
  • Zirconium
  • Zinc Oxide