Evaluation of portable Raman spectrometer with 1064 nm excitation for geological and forensic applications

Spectrochim Acta A Mol Biomol Spectrosc. 2012 Feb:86:320-7. doi: 10.1016/j.saa.2011.10.043. Epub 2011 Oct 20.

Abstract

The development of miniaturized Raman instrumentation is in demand for applications relevant to forensic, pharmaceutical and art analyses, as well as geosciences, and planetary exploration. In this study we report on evaluation of a portable dispersive Raman spectrometer equipped with 1064 nm laser excitation. Selected samples from geological, geobiological and forensic areas of interest have been studied from which the advantages, disadvantages and the analytical potential of the instrument are assessed based on a comparison with bench instrumentation and other portable Raman spectrometers using 785 nm excitation. It is demonstrated that the instrument operating with 1064 nm excitation has potential for expanding the number and types of samples that can be measured by miniaturized Raman spectroscopy without interfering fluorescence background emission. It includes inorganic and organic minerals, biomolecules within living lichen and endolithic cyanobacteria as well as drugs of abuse and explosives.

Publication types

  • Evaluation Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amber / analysis
  • Benzoates / analysis
  • Benzofurans / analysis
  • Calcium Oxalate / analysis
  • Explosive Agents / analysis
  • Forensic Sciences / methods*
  • Fossils
  • Geology / methods*
  • Illicit Drugs / analysis
  • Mercury Compounds / analysis
  • Minerals / analysis
  • Polystyrenes / analysis
  • Spectrum Analysis, Raman / instrumentation*
  • beta Carotene / analysis

Substances

  • Amber
  • Benzoates
  • Benzofurans
  • Explosive Agents
  • Illicit Drugs
  • Mercury Compounds
  • Minerals
  • Polystyrenes
  • beta Carotene
  • usnic acid
  • whewellite
  • Calcium Oxalate
  • mellitic acid
  • cinnabar