Nanostructured hydroxyapatite as filler for methacrylate-based root canal sealers

Int Endod J. 2012 Jan;45(1):63-7. doi: 10.1111/j.1365-2591.2011.01948.x. Epub 2011 Sep 8.

Abstract

Aim: To evaluate the effect of different concentrations of nanostructured hydroxyapatite on the radiopacity, flow and film thickness of an experimental root canal sealer.

Methodology: An experimental dual-cured root canal sealer was produced with a methacrylate-based co-monomer blend. Nanostructured hydroxyapatite/calcium tungstate solutions (ratios 10:90, 20:80, 30:70 and 40:60) were added to produce the sealer. Radiopacity was evaluated using a digital system and an aluminium step wedge (n=5). Flow and thickness tests were conducted in accordance with ISO 6876 (n=3). The data were analysed using one-way anova and Tukey's test (α=0.05).

Results: All groups had levels of radiopacity in accordance with ISO 6876. The flow of the experimental sealers was not significantly different (P=0.204). All groups had a film thickness in accordance with ISO 6876 and with no statistical difference (P = 0.654).

Conclusion: The addition of up to 40% HA(nano) to root canal sealers did not alter their radiopacity and film thickness.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Benzoyl Peroxide / chemistry
  • Biocompatible Materials / chemistry*
  • Calcium Compounds / chemistry
  • Camphor / analogs & derivatives
  • Camphor / chemistry
  • Contrast Media / chemistry
  • Durapatite / chemistry*
  • Humans
  • Materials Testing
  • Methacrylates / chemistry*
  • Nanostructures / chemistry*
  • Particle Size
  • Polyurethanes / chemistry
  • Resin Cements / chemistry
  • Root Canal Filling Materials / chemistry*
  • Silanes / chemistry
  • Sonication
  • Surface Properties
  • Temperature
  • Time Factors
  • Toluidines / chemistry
  • Tungsten Compounds / chemistry
  • Viscosity

Substances

  • Biocompatible Materials
  • Calcium Compounds
  • Contrast Media
  • Methacrylates
  • Polyurethanes
  • Resin Cements
  • Root Canal Filling Materials
  • Silanes
  • Toluidines
  • Tungsten Compounds
  • urethane dimethacrylate luting resin
  • 2,2-bis-(4-(2-methacryloxyethoxy)phenyl)propane
  • methacryloxypropyltrimethoxysilane
  • Camphor
  • calcium tungstate
  • Durapatite
  • N,N-bis(2-hydroxyethyl)-4-toluidine
  • camphorquinone
  • Benzoyl Peroxide