Micro-tensile bond strength and interfacial characterization of an adhesive bonded to dentin prepared by contemporary caries-excavation techniques

Dent Mater. 2011 Jun;27(6):552-62. doi: 10.1016/j.dental.2011.02.008. Epub 2011 Apr 13.

Abstract

Objectives: To evaluate the micro-tensile bond strength (μTBS) and interfacial characteristics of adhesive-dentin bonds produced after caries-removal with contemporary techniques.

Methods: Carious molars were cut at the base of the fissure, exposing 'sound' and 'carious' dentin at different spots. After caries-excavation, a composite was bonded using a 2-step self-etch adhesive. The μTBS was measured and the mode of fracture analyzed using a stereomicroscope and imaged by Feg-SEM, while additional non-fractured specimens were histologically analyzed after Masson's trichrome staining in order to identify potentially incompletely resin-enveloped collagen.

Results: μTBS to residual caries-excavated dentin was lower than to sound dentin. The different caries-removing techniques had a significant effect on the μTBS. Er:YAG laser guided by a LIF-feedback system (Kavo) resulted in the lowest μTBS (26.8% lower than to 'sound' dentin) and a distinct layer of incompletely resin-enveloped collagen at the interface. Although different degrees of collagen exposure were seen for other caries-removing techniques, such as a thick layer for CeraBur (Komet-Brasseler), some unprotected collagen areas for Cariex (Kavo), or completely resin-enveloped collagen for a tungsten-carbide-bur (Komet), the μTBS appeared not directly affected (10%, 16.6%, and 15.3% lower than to 'sound' dentin, respectively). Carisolv (MediTeam) resulted in the highest μTBS (only 1% reduction compared to that to 'sound' dentin), followed by the tungsten-carbide-bur aided by Caries Detector (Kuraray) (4.8% reduction). Enzymatic caries excavation using the experimental SFC-VIII (3M-ESPE) aided by a disposable plastic instrument resulted in a 19.4% reduction in μTBS as compared to that to 'sound' dentin.

Significance: The dentin bonding receptiveness depends to a large extent on the caries-excavation method employed.

Publication types

  • Comparative Study

MeSH terms

  • Azo Compounds
  • Collagen / ultrastructure
  • Coloring Agents
  • Composite Resins / chemistry
  • Crowns
  • Dental Bonding*
  • Dental Caries / therapy*
  • Dental Cavity Preparation / instrumentation
  • Dental Cavity Preparation / methods*
  • Dentin / ultrastructure*
  • Dentin-Bonding Agents / chemistry*
  • Eosine Yellowish-(YS)
  • Equipment Design
  • Glutamic Acid / chemistry
  • Humans
  • Lasers, Solid-State / therapeutic use
  • Leucine / chemistry
  • Lysine / chemistry
  • Materials Testing
  • Methyl Green
  • Microscopy, Electron, Scanning
  • Resin Cements / chemistry
  • Silicon Dioxide / chemistry
  • Stress, Mechanical
  • Surface Properties
  • Temperature
  • Tensile Strength
  • Time Factors
  • Tungsten Compounds / chemistry
  • Water / chemistry
  • Zirconium / chemistry

Substances

  • Azo Compounds
  • Carisolv
  • Clearfil SE Bond
  • Coloring Agents
  • Composite Resins
  • Dentin-Bonding Agents
  • Resin Cements
  • Tungsten Compounds
  • Z100 composite resin
  • trichrome stain
  • Water
  • tungsten carbide
  • Glutamic Acid
  • Silicon Dioxide
  • Methyl Green
  • Collagen
  • Zirconium
  • Leucine
  • Lysine
  • Eosine Yellowish-(YS)