Development of a cryogenic stage for an ion-milling instrument

J Electron Microsc (Tokyo). 2011;60(1):25-7. doi: 10.1093/jmicro/dfq069. Epub 2010 Oct 8.

Abstract

A specimen-cooling device has been designed, manufactured and integrated into a commercial ion-milling instrument for transmission electron microscopy. The instrument enables us to prepare section specimens of tin-plated Cu without forming intermetallic compound particles and/or voids. The results show that cooling of specimen during ion-milling process is necessary for fine structure investigations of low melting temperature materials.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Cold Temperature
  • Copper / chemistry*
  • Ions
  • Microscopy, Electron, Transmission / methods*
  • Specimen Handling / instrumentation*
  • Tin / chemistry

Substances

  • Ions
  • Tin
  • Copper