Abstract
Mixtures of lipids and phospholipids were separated by centrifugally accelerated thin-layer chromatography on a preparative scale (300-500 mg lipid mixture per run). The isolated lipids and phospholipids were identified by 1H and 13C NMR spectroscopy and their fatty acid composition was determined by GLC and GLC-MS of their methyl esters.
Publication types
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Research Support, Non-U.S. Gov't
MeSH terms
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Centrifugation
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Chromatography, Thin Layer / methods*
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Fatty Acids / analysis
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Gas Chromatography-Mass Spectrometry
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Hydrolysis
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Lipids / chemistry
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Lipids / isolation & purification*
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Magnetic Resonance Spectroscopy
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Methylation
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Phospholipids / chemistry
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Phospholipids / isolation & purification*
Substances
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Fatty Acids
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Lipids
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Phospholipids