Combination treatment of tribochemical treatment and phosphoric acid ester monomer of zirconia ceramics enhances the bonding durability of resin-based luting cements

Dent Mater J. 2010 May;29(3):316-23. doi: 10.4012/dmj.2009-099. Epub 2010 May 18.

Abstract

The aim of the present study was to evaluate the bonding durability of resin-based luting cement to partially stabilized tetragonal zirconia (Y-TZP) achieved by combination treatment of tribochemical (TBC) treatment and two different phosphate acid ester monomers. Two phosphate acid ester monomers (EP: Epricord opaque primer, AZ: AZ primer) were applied to each surface modification followed by application of resin-based luting cement (Rely-X ARC). Bonding specimens were placed in deionized water at 37 degrees C and stored for 24 h. The other groups were subjected to 30,000 cycles of a thermal stress for the durability test. Shear bond tests were done using a universal testing machine at 1 mm/min. Shear bond strengths of combination treatments using EP and AZ on TBC treatment after thermal stress showed no significant difference (p>0.05) compared with those of storage after 24 h. Combination treatment using phosphoric acid ester monomer could achieve a durable bond.

MeSH terms

  • Bisphenol A-Glycidyl Methacrylate
  • Composite Resins
  • Dental Bonding*
  • Dental Etching / methods*
  • Dental Porcelain*
  • Dental Stress Analysis
  • Friction
  • Materials Testing
  • Methacrylates
  • Organophosphates*
  • Phosphonoacetic Acid / analogs & derivatives
  • Polyethylene Glycols
  • Polymethacrylic Acids
  • Resin Cements*
  • Shear Strength
  • Yttrium
  • Zirconium

Substances

  • 6-methacryloyloxyhexyl phosphonoacetate
  • Composite Resins
  • Methacrylates
  • Organophosphates
  • Polymethacrylic Acids
  • RelyX ARC
  • Resin Cements
  • epricord
  • yttria stabilized tetragonal zirconia
  • Dental Porcelain
  • Polyethylene Glycols
  • Bisphenol A-Glycidyl Methacrylate
  • Yttrium
  • Zirconium
  • Phosphonoacetic Acid