Abstract
Here we provide new experimental results on multicomponent reactions of amines with aldehydes and H(2)S in the directed synthesis of functionally-substituted 1,3-thiazetidines, 1,3,5-dithiazinanes, 1,3,5-thiadiazinanes, 1,5-dithia-3,7-diazacyclooctanes, and thioaza macrocycles. X-ray analysis gave insight into the structure of the synthesized compounds. New kinds of multicomponent reactions (MCR) have been discovered and characterized.
MeSH terms
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Aldehydes / chemistry*
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Amines / chemistry*
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Aza Compounds / chemical synthesis*
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Aza Compounds / chemistry
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Chemistry, Organic / methods*
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Crystallography, X-Ray
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Heterocyclic Compounds / chemical synthesis*
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Heterocyclic Compounds / chemistry
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Hydrazines / chemistry
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Hydrogen Sulfide / chemistry*
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Macrocyclic Compounds / chemical synthesis*
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Macrocyclic Compounds / chemistry
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Molecular Conformation
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Phenols / chemical synthesis
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Phenols / chemistry
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Temperature
Substances
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Aldehydes
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Amines
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Aza Compounds
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Heterocyclic Compounds
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Hydrazines
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Macrocyclic Compounds
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Phenols
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Hydrogen Sulfide