Effect of primer treatment on bonding of resin cements to zirconia ceramic

Dent Mater. 2010 May;26(5):426-32. doi: 10.1016/j.dental.2009.11.159. Epub 2010 Jan 25.

Abstract

Objectives: To evaluate and compare bond strengths of different primers and resin cements to silica-based and zirconia ceramics.

Methods: Silica-based and zirconia ceramic specimens were ground flat with #600-grit SiC paper. The ceramic surfaces were airborne-particle abraded and then divided into 11 groups of seven each: untreated (control); and conditioned with one of the six primers in combination with a resin cement from the same manufacturer as follows: Bistite II/Tokuso Ceramic Primer, Linkmax/GC Ceramic Primer, RelyX ARC/RelyX Ceramic Primer, Panavia F 2.0/Clearfil Ceramic Primer, and Resicem/Shofu Porcelain Primer and Resicem/AZ Primer. Stainless steel rods were bonded to the ceramic surfaces using one of the five resin cements. After 24-h water storage, the tensile bond strengths were tested using a universal testing machine and failure modes were examined.

Results: Conditioning with primers containing a silane coupling agent (all the primers except AZ Primer) significantly enhanced bond strengths of resin cements to silica-based ceramic. For zirconia ceramic, Resicem/AZ Primer exhibited significantly higher bond strength than the other groups except Panavia F 2.0/Clearfil Ceramic Primer. The predominant failure mode of the groups conditioned with primers containing a phosphonic acid monomer (AZ Primer) or a phosphate ester monomer (Clearfil Ceramic Primer and Tokuso Ceramic Primer) was cohesive failure in cements whereas that with the other primers was adhesive failure at the zirconia surfaces.

Significance: The use of primers containing a silane coupling agent improved resin bonding to silica-based ceramic. On the other hand, the use of primers containing a phosphonic acid monomer or a phosphate ester monomer improved resin bonding to zirconia ceramic.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Analysis of Variance
  • Dental Bonding / methods*
  • Dental Porcelain*
  • Dental Stress Analysis
  • Materials Testing
  • Methacrylates
  • Organophosphonates
  • Phosphonoacetic Acid / analogs & derivatives
  • Resin Cements*
  • Silanes
  • Silicon Dioxide
  • Statistics, Nonparametric
  • Tensile Strength
  • Yttrium
  • Zirconium

Substances

  • 6-methacryloyloxyhexyl phosphonoacetate
  • Methacrylates
  • Organophosphonates
  • Resin Cements
  • Silanes
  • yttria stabilized tetragonal zirconia
  • Dental Porcelain
  • Yttrium
  • Silicon Dioxide
  • methacryloyloxydecyl dihydrogen phosphate
  • Zirconium
  • Phosphonoacetic Acid