Synthesis of acetal protected building blocks using flow chemistry with flow I.R. analysis: preparation of butane-2,3-diacetal tartrates

Catherine F Carter; Ian R Baxendale; Matthew O'Brien; John B J Pavey; Steven V Ley

doi:10.1039/b917289k

Synthesis of acetal protected building blocks using flow chemistry with flow I.R. analysis: preparation of butane-2,3-diacetal tartrates

Org Biomol Chem. 2009 Nov 21;7(22):4594-7. doi: 10.1039/b917289k. Epub 2009 Sep 28.

Authors

Catherine F Carter¹, Ian R Baxendale, Matthew O'Brien, John B J Pavey, Steven V Ley

Affiliation

¹ Department of Chemistry, Innovative Technology Centre, University of Cambridge, Lensfield Road, Cambridge, CB2 1EW, UK.

PMID: 19865693
DOI: 10.1039/b917289k

Abstract

The syntheses of butane-2,3-diacetal protected tartrate derivatives are described using continuous flow processing techniques with in-line purification and I.R. analytical protocols.

Publication types

Research Support, Non-U.S. Gov't

MeSH terms

Acetals / chemical synthesis*
Acetals / chemistry
Biological Products / chemical synthesis
Biological Products / chemistry
Esters / chemical synthesis
Esters / chemistry
Rheology / instrumentation
Rheology / methods*
Spectroscopy, Fourier Transform Infrared
Tartrates / chemical synthesis*
Tartrates / chemistry

Substances

Acetals
Biological Products
Esters
Tartrates