High-precision heteronuclear 2D NMR experiments using 10-ppm spectral window to resolve carbon overlap

Bruno Vitorge; Stefan Bieri; Munir Humam; Philippe Christen; Kurt Hostettmann; Orlando Muñoz; Sandra Loss; Damien Jeannerat

doi:10.1039/b820478k

High-precision heteronuclear 2D NMR experiments using 10-ppm spectral window to resolve carbon overlap

Chem Commun (Camb). 2009 Feb 28:(8):950-2. doi: 10.1039/b820478k. Epub 2009 Jan 20.

Authors

Bruno Vitorge¹, Stefan Bieri, Munir Humam, Philippe Christen, Kurt Hostettmann, Orlando Muñoz, Sandra Loss, Damien Jeannerat

Affiliation

¹ Department of Organic Chemistry, University of Geneva, Quai Ernest-Ansermet 30, CH-1211, Geneva 4, Switzerland.

PMID: 19214326
DOI: 10.1039/b820478k

Abstract

The acquisition of a complementary heteronuclear 2D NMR experiment with 10-ppm carbon window allows chemists to improve by a factor 20-25 the spectral resolution and determine carbon chemical shifts with five figures from 2D spectra.

Publication types

Research Support, Non-U.S. Gov't

MeSH terms

Biological Products / chemistry
Carbon / chemistry*
Carbon Isotopes
Molecular Structure
Nuclear Magnetic Resonance, Biomolecular*

Substances

Biological Products
Carbon Isotopes
Carbon