Effect of simulated pulpal pressure on self-adhesive cements bonding to dentin

Dent Mater. 2008 Sep;24(9):1156-63. doi: 10.1016/j.dental.2008.01.005. Epub 2008 Mar 4.

Abstract

Objectives: To evaluate the bonding effectiveness of self-adhesive luting cements to dentin in the presence of simulated hydrostatic intrapulpal pressure (PP).

Methods: Thirty composite overlays (Aelite All Purpose Body) were luted to deep-coronal dentin surfaces using four self-adhesive resin cements (Rely X Unicem, G-Cem, Multilink Sprint, Bis-Cem) and one total-etch system (Calibra). Half of the specimens resin cements were applied under a PP of 15 cm H2O. After storage in a moist condition for 1 month (37 degrees C, 100% relative humidity), specimens were sectioned into microtensile beams (1mm2) and stressed to failure with the microtensile bond strength test (microTBS). Data were statistically analyzed with Kruskal-Wallis ranking (p<0.05) and Mann-Whitney tests (p<0.001). The fracture pattern was evaluated under SEM.

Results: Bond strength of Calibra fell significantly when PP was applied during bonding (p<0.05). Rely X Unicem and Bis-Cem performed better under PP. No significant differences for Multilink Sprint and G-Cem bonded specimens were recorded with or without PP.

Significance: Simulated PP influences the adhesive performance of resinous cements. The predominance of acid-base reactions or radical polymerization may explain the different behavior of self-adhesive cements when changing substrate wetness. The application of constant intrapulpal perfusion should be considered when simulating luting procedures in vitro.

MeSH terms

  • Composite Resins / chemistry
  • Dental Bonding*
  • Dental Pulp / physiology*
  • Dentin / ultrastructure*
  • Dentin-Bonding Agents / chemistry*
  • Humans
  • Humidity
  • Hydrostatic Pressure
  • Materials Testing
  • Methacrylates / chemistry
  • Microscopy, Electron, Scanning
  • Partial Pressure
  • Polyethylene Glycols / chemistry
  • Polymethacrylic Acids / chemistry
  • Resin Cements / chemistry
  • Stress, Mechanical
  • Surface Properties
  • Temperature
  • Tensile Strength
  • Time Factors

Substances

  • Aelite LS
  • Calibra
  • Composite Resins
  • Dentin-Bonding Agents
  • G-Cem resin cement
  • Methacrylates
  • Polymethacrylic Acids
  • Rely X Unicem
  • Resin Cements
  • multilink adhesive system
  • triethylene glycol dimethacrylate
  • Polyethylene Glycols
  • hydroxyethyl methacrylate