Surface conditioning of a composite used for inlay/onlay restorations: effect on muTBS to resin cement

J Adhes Dent. 2007 Dec;9(6):495-8.

Abstract

Purpose: To assess the effect of the composite surface conditioning on the microtensile bond strength of a resin cement to a composite used for inlay/onlay restorations.

Materials and methods: Forty-two blocks (6 x 6 x 4 mm) of a microfilled composite (Vita VMLC) were produced and divided into 3 groups (N = 14) by composite surface conditioning methods: Gr1--etching with 37% phosphoric acid, washing, drying, silanization; Gr2--air abrasion with 50-lm Al203 particles, silanization; Gr3--chairside tribochemical silica coating (CoJet System), silanization. Single-Bond (one-step adhesive) was applied on the conditioned surfaces and the two resin blocks treated with the same method were cemented using RelyX ARC (dual-curing resin cement). The specimens were stored for 7 days in water at 37 degrees C and then sectioned to produce nontrimmed beam samples, which were submitted to microtensile bond strength testing (muTBS). For statistical analysis (one-way ANOVA and Tukey's test, alpha = 0.05), the means of the beam samples from each luted specimen were calculated (n = 7).

Results: muTBS values (MPa) of Gr2 (62.0 +/- 3.9a) and Gr3 (60.5 +/- 7.9a) were statistically similar to each other and higher than Gr1 (38.2 +/- 8.9b). The analysis of the fractured surfaces revealed that all failures occurred at the adhesive zone.

Conclusion: Conditioning methods with 50-lm Al203 or tribochemical silica coating allowed bonding between resin and composite that was statistically similar and stronger than conditioning with acid etching.

MeSH terms

  • Acid Etching, Dental
  • Adhesiveness
  • Aluminum Oxide / chemistry
  • Bisphenol A-Glycidyl Methacrylate / chemistry
  • Composite Resins / chemistry*
  • Dental Bonding*
  • Dental Etching
  • Dentin-Bonding Agents / chemistry
  • Humans
  • Inlays*
  • Materials Testing
  • Phosphoric Acids / chemistry
  • Polyethylene Glycols / chemistry
  • Polymethacrylic Acids / chemistry
  • Resin Cements / chemistry*
  • Silanes / chemistry
  • Silicon Dioxide / chemistry
  • Stress, Mechanical
  • Surface Properties
  • Temperature
  • Tensile Strength
  • Water / chemistry

Substances

  • Composite Resins
  • Dentin-Bonding Agents
  • ESPE bonding system
  • Phosphoric Acids
  • Polymethacrylic Acids
  • RelyX ARC
  • Resin Cements
  • Silanes
  • single bond
  • Water
  • Polyethylene Glycols
  • Bisphenol A-Glycidyl Methacrylate
  • Silicon Dioxide
  • phosphoric acid
  • Aluminum Oxide