Abstract
Objective:
To search for the method used in refining Xiaoyao Pill by macroporous adsorption resin, 12 types of macroporous adsorption resin were optimized.
Method:
Static and dynamic adsorption test and de-adsorption test were carried out to screen the best macroporous resin. The single factor test was applied to optimize the manipulation parameters of macroporous resin.
Result:
The macroporous resin D-101-1 possessed the strongest adsorption ability, in addition to an easy de-adsorption property.
Conclusion:
The D-101-1 type macroporous adsorption resin shows better comprehensive adsorption property. It is available for the refine Xiaoyao Pill.
MeSH terms
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Adsorption
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Benzoates / analysis
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Benzoates / isolation & purification
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Bridged-Ring Compounds / analysis
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Bridged-Ring Compounds / isolation & purification
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Coumaric Acids / analysis
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Coumaric Acids / isolation & purification
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Drug Combinations
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Drugs, Chinese Herbal / chemistry*
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Glucosides / analysis
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Glucosides / isolation & purification
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Glycyrrhetinic Acid / analysis
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Glycyrrhetinic Acid / isolation & purification
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Monoterpenes
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Oleanolic Acid / analogs & derivatives
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Oleanolic Acid / analysis
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Oleanolic Acid / isolation & purification
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Plants, Medicinal / chemistry*
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Resins, Synthetic*
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Saponins / analysis
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Saponins / isolation & purification
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Tablets
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Technology, Pharmaceutical / methods*
Substances
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Benzoates
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Bridged-Ring Compounds
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Coumaric Acids
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Drug Combinations
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Drugs, Chinese Herbal
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Glucosides
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Monoterpenes
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Resins, Synthetic
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Saponins
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Tablets
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xiaoyao
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peoniflorin
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Oleanolic Acid
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ferulic acid
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Glycyrrhetinic Acid
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saikosaponin D