Three-dimensional visualization of the inner structure of single crystals by step-scanning white X-ray section topography

J Synchrotron Radiat. 2006 Nov;13(Pt 6):484-8. doi: 10.1107/S090904950603384X. Epub 2006 Oct 18.

Abstract

Visualization of the three-dimensional distribution of the crystal defects of large single crystals of calcium fluoride has been demonstrated by white X-ray section topography using sheet-like X-rays (BL28B2 at SPring-8). An image of the three-dimensional distribution of the crystal defects was reconstructed by stacking section topographs, which expressed the images of cross sections of the sample. The section topographs were recorded using a CMOS flat-panel imager or a CCD detector combined with scintillator (Gd(2)O(2)S:Tb) and relay lens system. The section topographs were measured by repeating cycles of exposure and sample translation along the direction perpendicular to the top face of the sample. Using high-brilliance and high-energy white X-rays ( approximately 60 keV) efficiently, visualization of the three-dimensional structure of subgrains of a sample of up to 60 mm in diameter was achieved. Furthermore, the three-dimensional distribution of the glide plane in the crystal was visualized by reconstructing the linear contrast of the glide plane.

MeSH terms

  • Calcium Fluoride / chemistry*
  • Crystallography, X-Ray / methods*
  • Image Interpretation, Computer-Assisted / methods*
  • Imaging, Three-Dimensional
  • Molecular Conformation
  • Tomography, Optical / methods*

Substances

  • Calcium Fluoride