Simultaneous determination of cinnamaldehyde, eugenol and paeonol in traditional Chinese medicinal preparations by capillary GC-FID

Chem Pharm Bull (Tokyo). 2006 Jan;54(1):114-6. doi: 10.1248/cpb.54.114.

Abstract

A capillary GC method was established for simultaneous determination of cinnamaldehyde (CNMD), eugenol (EL) and paeonol (PL) in two traditional Chinese herbal medicinal preparations, Weitongding tablet (WTDT) and Guifu Dihuang pill (GDHP). The assays were based on a programmed temperature GC in a 30 m x 0.53 mm capillary column with nitrogen as carrier and FID detector. Good linearities were obtained over ranges of 0.45-452 mg/l CNMD, 0.31-625 mg/l EL and 0.30-610 mg/l PL, respectively. The spike recoveries were within 84-111%.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Acetophenones / analysis*
  • Acrolein / analogs & derivatives*
  • Acrolein / analysis
  • Chromatography, Gas
  • Chromatography, High Pressure Liquid
  • Drugs, Chinese Herbal / analysis*
  • Eugenol / analysis*
  • Indicators and Reagents
  • Reference Standards
  • Reproducibility of Results
  • Tablets

Substances

  • Acetophenones
  • Drugs, Chinese Herbal
  • Indicators and Reagents
  • Tablets
  • paeonol
  • Eugenol
  • Acrolein
  • cinnamaldehyde