Rapid pulse length determination in high-resolution NMR

Peter S C Wu; Gottfried Otting

doi:10.1016/j.jmr.2005.05.018

Rapid pulse length determination in high-resolution NMR

J Magn Reson. 2005 Sep;176(1):115-9. doi: 10.1016/j.jmr.2005.05.018.

Authors

Peter S C Wu¹, Gottfried Otting

Affiliation

¹ Research School of Chemistry, Australian National University, Canberra, ACT 0200, Australia.

PMID: 15972263
DOI: 10.1016/j.jmr.2005.05.018

Abstract

The 90 degrees (1H) pulse length can be determined in a single scan using a simple homo-gated decoupling/nutation experiment. We show that the method is fast, accurate and readily amenable to automation.

Publication types

Research Support, Non-U.S. Gov't

MeSH terms

Animals
Chickens
Muramidase / chemistry*
Nuclear Magnetic Resonance, Biomolecular / methods*

Substances

Muramidase