A new X-ray spectrometer with large focusing crystal analyzer

J Synchrotron Radiat. 2005 Jul;12(Pt 4):448-54. doi: 10.1107/S0909049505007843. Epub 2005 Jun 15.

Abstract

A new focusing spectrometer employing Johann geometry has been built and permanently installed at the wiggler beamline W1 at the Hamburger Synchrotron Strahlungslabor (HASYLAB) am Deutschen Elektronen Synchrotron (DESY). It is now available for user operation. The design of the spectrometer is optimized for the use of a large source spot size at the DORIS storage ring as well as for simple operation and robustness under user-mode conditions. Nevertheless, the ideal source for enlarging the number of possible applications in the future would be an undulator at one of the PETRA III beamlines. In the following the spectrometer design is described and boundary conditions such as the available energy range for future experiments are discussed. Two benchmark experiments, resonant inelastic X-ray scattering (RIXS) and X-ray absorption fluorescence spectroscopy (XAFS), on samples with complicated matrices demonstrate the performance of the new instrument.

Publication types

  • Evaluation Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Calibration
  • Computer-Aided Design*
  • Crystallography, X-Ray / instrumentation*
  • Crystallography, X-Ray / methods
  • Equipment Design
  • Equipment Failure Analysis
  • Photons
  • Spectrometry, X-Ray Emission / instrumentation*
  • Spectrometry, X-Ray Emission / methods