NMR study on (+/-)-1-[3-(2-methoxyphenoxy)-2-hydroxypropyl]-4-[(2,6-dimethylphenyl)aminocarbonylmethyl]piperazine dihydrochloride salt

Bingjie Qin; Jimao Lin; Zhenguang Lin; Yun Xue; Huixue Ren

doi:10.1016/j.saa.2004.04.028

NMR study on (+/-)-1-[3-(2-methoxyphenoxy)-2-hydroxypropyl]-4-[(2,6-dimethylphenyl)aminocarbonylmethyl]piperazine dihydrochloride salt

Spectrochim Acta A Mol Biomol Spectrosc. 2005 Feb;61(4):665-71. doi: 10.1016/j.saa.2004.04.028.

Authors

Bingjie Qin¹, Jimao Lin, Zhenguang Lin, Yun Xue, Huixue Ren

Affiliation

¹ School of Chemistry and Chemical Engineering, Shandong University, Jinan 250100, PR China.

PMID: 15649799
DOI: 10.1016/j.saa.2004.04.028

Abstract

(+/-)-1-[3-(2-Methoxyphenoxy)-2-hydroxypropyl]-4-[(2,6-dimethylphenyl)aminocarbonylmethyl]piperazine dihydrochloride salt was studied spectroscopically. Complete NMR assignments for dihydrochloride salt were made using DEPT, H-H COSY, as well as HMQC and HMBC heteronuclear correlation techniques.

MeSH terms

Carbon / chemistry
Magnetic Resonance Spectroscopy / methods*
Models, Chemical
Piperazine
Piperazines / analysis
Piperazines / chemistry*
Protons
Spectrophotometry / methods*

Substances

1-(3-(2-methoxyphenoxy)-2-hydroxypropyl)-4-((2,6-dimethylphenyl)aminocarbonylmethyl)piperazine dihydrochloride salt
Piperazines
Protons
Piperazine
Carbon