Effects of additional and extended acid etching on bonding to caries-affected dentine

Eur J Oral Sci. 2004 Oct;112(5):458-64. doi: 10.1111/j.1600-0722.2004.00159.x.

Abstract

This study evaluated the effects of additional and extended acid etching on microtensile bond strength ( micro TBS) of two adhesive systems to sound (SD) and caries-affected dentine (CAD). Flat surfaces of CAD surrounded by SD of 36 extracted carious third molars were assigned to four treatments (i): self-etching adhesive system (Clearfil SE Bond) applied to dentine surfaces following manufacturer's instructions (MI); (ii) after additional etching for 15 s (35% phosphoric acid, PA); (iii) total-etch one-bottle adhesive (Single Bond) applied to dentine surfaces following MI; or (iv), after etching for 45 s with PA. Composite 'blocks' were built on bonded surfaces and restored teeth were vertically sectioned to obtain bonded slices of 0.7 mm thick. Slices were trimmed to create hourglass-shaped specimens (cross-sectional area of 1 mm(2)), which were tested under tension in a universal testing machine. Additional CAD and SD samples were prepared for scanning electron microscopy observations. Additional and extended etching significantly increased micro TBS to CAD; however, micro TBS of both adhesives to CAD were significantly lower than to SD. Additional and extended etching can improve bonding to CAD; however, adhesives applied on SD showed the best results for bonding.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Acid Etching, Dental / methods*
  • Bisphenol A-Glycidyl Methacrylate / chemistry
  • Composite Resins / chemistry
  • Dental Bonding*
  • Dental Caries / pathology*
  • Dentin / ultrastructure*
  • Dentin-Bonding Agents / chemistry*
  • Humans
  • Materials Testing
  • Microscopy, Electron, Scanning
  • Phosphoric Acids / chemistry
  • Resin Cements / chemistry
  • Surface Properties
  • Tensile Strength
  • Time Factors

Substances

  • Clearfil SE Bond
  • Composite Resins
  • Dentin-Bonding Agents
  • Phosphoric Acids
  • Resin Cements
  • single bond
  • Bisphenol A-Glycidyl Methacrylate