Facile characterization of polymer-supported reagents using cross polarization magic angle spinning method in solid state 13C-NMR

Kazuaki Shikii; Hiroko Seki; Kentaro Yamaguchi; Wannaporn Disadee; Toshiko Watanabe; Tsutomu Ishikawa

doi:10.1248/cpb.52.864

Facile characterization of polymer-supported reagents using cross polarization magic angle spinning method in solid state 13C-NMR

Chem Pharm Bull (Tokyo). 2004 Jul;52(7):864-5. doi: 10.1248/cpb.52.864.

Authors

Kazuaki Shikii¹, Hiroko Seki, Kentaro Yamaguchi, Wannaporn Disadee, Toshiko Watanabe, Tsutomu Ishikawa

Affiliation

¹ Chemical Analysis Center, Chiba University, Japan.

PMID: 15256711
DOI: 10.1248/cpb.52.864

Abstract

Polymer-supported (PS) reagents can be easily characterized using a cross polarization magic angle spinning method in solid state (13)C-NMR. The technique was applied to the characterization of PS-dimethylimidazolidinone, analogue to potential heterogeneous dehydrating agent.

MeSH terms

Carbon Isotopes
Magnetic Resonance Spectroscopy / methods*
Polymers / analysis*
Polymers / classification*

Substances

Carbon Isotopes
Polymers