Reactive fibre reinforced glass ionomer cements

Biomaterials. 2003 Aug;24(17):2901-7. doi: 10.1016/s0142-9612(03)00130-3.

Abstract

The mechanical properties of glass ionomer cements used in restorative dentistry reinforced by chopped glass fibres were investigated. Reactive glass fibres with a composition in the system SiO(2)-Al(2)O(3)-CaF(2)-Na(3)AlF(6) and a thickness of 26 microm were drawn by a bushing process. The manufacturing parameters were optimized with respect to maximum strength of the glass fibre reinforced ionomer cements. Powder to liquid ratio, pre-treatment of the glass, grain size distribution and fibre volume fraction were varied. Glass fibre and cement were characterized by X-ray diffraction, transmission electron microscopy and energy dispersive spectroscopy techniques, respectively. The highest flexural strength of the reinforced cement (15.6 MPa) was found by compounding 20 vol% reactive fibres and extending the initial dry gelation period up to 30 min. Microscopic examination of the fractured cements indicated a distinct reactive layer at the fibre surface. A pronounced fibre pull out mode gives rise to an additional work-of-fracture contributed by pulling the fibres out of the fracture surface.

Publication types

  • Comparative Study
  • Evaluation Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Compressive Strength
  • Elasticity
  • Glass / chemistry*
  • Glass Ionomer Cements / chemical synthesis
  • Glass Ionomer Cements / chemistry*
  • Glass Ionomer Cements / classification
  • Manufactured Materials
  • Materials Testing*
  • Stress, Mechanical
  • Surface Properties
  • Tensile Strength

Substances

  • Glass Ionomer Cements
  • fiberglass