The in vitro dentin bond strengths of two adhesive systems in class I cavities of human molars

J Adhes Dent. 2002 Spring;4(1):31-9.

Abstract

Purpose: The purpose of this study was to evaluate the in vitro dentin bond strengths of two dentin bonding systems in Class I cavities following fatigue load cycling (FLC) with thermal cycling (TC).

Materials and methods: Class I cavities were prepared in 12 human molars and restored with either Clearfil SE Bond (SE) and Clearfil AP-X resin composite (AP-X) or Single Bond (SB)/AP-X according to the manufacturers' instructions. After water storage for 1 week, untreated controls and test samples were subjected to 50,000 FLC with TC from 5 degrees C to 55 degrees C for 625 cycles and stored in water for 1 week. Microtensile bond strength (MTBS) tests were measured on the floor of the cavities at a crosshead speed of 1 mm/min. Data were statistically analyzed using one- and two-way ANOVA and Fisher's PLSD test at a 5% level of significance.

Results: The MPa results were: SE 30.5+/-12.8 (control) and 23.2+/-10.8 (50,000 FLC); SB 5.1+/-9.2 (control) and 4.7+/-5.7 (50,000 FLC). Bond strengths were not statistically significantly affected by FLC (p > 0.05); however, they were influenced by the bonding system (p < 0.05). The MTBS of SE was significantly higher than that of SB (p < 0.05) under FLC and TC test conditions. Over half of the SB specimens debonded during sample preparation, showing blister-like structures, suggesting that an over-wet phenomenon occurred on the cavity floor.

Conclusion: SE produced excellent dentin bonds that were much stronger than those produced by SB, which was shown to be a technique-sensitive bonding system.

MeSH terms

  • Acid Etching, Dental
  • Analysis of Variance
  • Bisphenol A-Glycidyl Methacrylate / chemistry
  • Composite Resins / chemistry
  • Dental Bonding*
  • Dental Cavity Preparation / classification*
  • Dentin / ultrastructure*
  • Dentin-Bonding Agents / chemistry*
  • Humans
  • Materials Testing
  • Methacrylates / chemistry
  • Microscopy, Electron, Scanning
  • Molar
  • Resin Cements / chemistry
  • Statistics as Topic
  • Stress, Mechanical
  • Surface Properties
  • Temperature
  • Tensile Strength
  • Thermodynamics
  • Water / chemistry
  • Weight-Bearing

Substances

  • Clearfil AP-X
  • Clearfil SE Bond
  • Composite Resins
  • Dentin-Bonding Agents
  • Methacrylates
  • Resin Cements
  • single bond
  • Water
  • Bisphenol A-Glycidyl Methacrylate