Determination of manganese in herbal medicine samples by slurry-sampling electrothermal atomic absorption spectrometry with a metal tube atomizer

Anal Bioanal Chem. 2002 Jun;373(3):205-8. doi: 10.1007/s00216-002-1303-1. Epub 2002 May 4.

Abstract

An ultrasonic slurry-sampling electrothermal atomic absorption spectrometry with a molybdenum tube atomizer has been developed for the determination of manganese in herbal medicine samples. Ten percent glycerol solution was used as the slurry medium. The optimum pyrolysis temperature was 400 degrees C. The detection limit was 69 fg (3xS/N). Matrix element interference was checked and it was found that glycerol as a chemical modifier eliminated the interference. The amounts of manganese in herbal medicines determined by the proposed method are in good accordance with those measured in dissolved acid-digested samples. The method enables rapid calibration, and simple and rapid analysis of manganese in herbal medicine samples at low cost.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Herbal Medicine*
  • Hot Temperature
  • Manganese / analysis*
  • Pharmaceutical Preparations / chemistry*
  • Reproducibility of Results
  • Sensitivity and Specificity
  • Spectrophotometry, Atomic / methods*

Substances

  • Pharmaceutical Preparations
  • Manganese