Laser pyrolysis fabrication of ferromagnetic gamma'-Fe4N and FeC nanoparticles

J Appl Phys. 2000 May 1;87(9 Pt 2):5642-4. doi: 10.1063/1.373419.

Abstract

Using the laser pyrolysis method, single phase gamma'-Fe4N nanoparticles were prepared by a two step method involving preparation of nanoscale iron oxide and a subsequent gas-solid nitridation reaction. Single phase Fe3C and Fe7C3 could be prepared by laser pyrolysis from Fe(CO)5 and 3C2H4 directly. Characterization techniques such as XRD, TEM and vibrating sample magnetometer were used to measure phase structure, particle size and magnetic properties of these nanoscale nitride and carbide particles.

Publication types

  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Carbon Compounds, Inorganic*
  • Iron Compounds*
  • Lasers*
  • Magnetics*
  • Nanotechnology*
  • Nitrogen Compounds*
  • Particle Size
  • Temperature
  • X-Ray Diffraction

Substances

  • Carbon Compounds, Inorganic
  • Iron Compounds
  • Nitrogen Compounds