Laboratory strength of glass ionomer and zinc phosphate cements

J Prosthodont. 2001 Sep;10(3):140-7. doi: 10.1111/j.1532-849x.2001.00140.x.

Abstract

Purpose: The present in vitro study examined 3 mechanical properties, namely compressive, flexural, and diametral tensile strength, of various commercially available cements and core materials as a function of time after mixing.

Materials and methods: The examined materials were 2 cermet cements (Ketac Silver [ESPE, Seefeld, Germany] and Chelon Silver [ESPE]), 1 metal-reinforced glass ionomer cement (Miracle Mix [GC Dental Industrial Corp, Tokyo, Japan]), 2 conventional glass ionomer cements (Ketac Bond [ESPE] and Ketac Cem [ESPE]), 1 standard cure zinc phosphate cement (Harvard Cement [Richter and Hoffmann, Berlin, Germany]), and 1 zinc phosphate cement with the addition of 30% silver amalgam alloy powder (Harvard Cement 70% with Dispersalloy 30% [Richter and Hoffmann/Johnson and Johnson, East Windsor, NJ]). Properties were measured using a universal testing machine at 15 minutes, 1 hour, and 24 hours after first mixing.

Results: Compressive strengths varied widely between the 3 times of measurement from 5.8 +/- 6.6 MPa for Ketac Cem to 144.3 +/- 10.2 MPa for Ketac Silver. Twenty-four hours after mixing, the Bonferroni test showed significant (p <or= .01) differences between Ketac Silver and all other materials tested. Diametral tensile strengths ranged widely from 4.4 +/- 0.9 MPa for Ketac Cem to 11.5 +/- 2.2 MPa for Chelon Silver. At 15 minutes, 1 hour, and 24 hours after first mixing, the analysis of variance did not show any significant differences between Ketac Silver, Chelon Silver, and Miracle Mix. The 3-point flexural strength of Ketac Silver showed, at 15 minutes with 13.5 +/- 3.9 MPa and at 24 hours with 27.2 +/- 7.4 MPa, the highest values.

Conclusions: Setting time influences the mechanical properties of the materials tested in this study. Ketac Silver, a glass ionomer cement reinforced with sintered glass-silver particles, showed the highest mechanical properties of the examined materials.

Publication types

  • Comparative Study

MeSH terms

  • Analysis of Variance
  • Cermet Cements / chemistry
  • Compressive Strength
  • Dental Alloys / chemistry
  • Dental Amalgam / chemistry
  • Dental Stress Analysis / instrumentation
  • Glass Ionomer Cements / chemistry*
  • Hardness
  • Humans
  • Magnesium Oxide / chemistry
  • Materials Testing
  • Pliability
  • Polycarboxylate Cement / chemistry
  • Silver / chemistry
  • Silver Compounds / chemistry
  • Statistics as Topic
  • Stress, Mechanical
  • Surface Properties
  • Tensile Strength
  • Time Factors
  • Zinc Oxide / chemistry
  • Zinc Phosphate Cement / chemistry*

Substances

  • Cermet Cements
  • Dental Alloys
  • Glass Ionomer Cements
  • Polycarboxylate Cement
  • Silver Compounds
  • Ketac-Bond
  • Miracle Mix
  • Chelon Silver
  • Dispersalloy
  • Magnesium Oxide
  • Silver
  • Zinc Phosphate Cement
  • Dental Amalgam
  • Harvard Cement
  • Ketac-cem
  • Zinc Oxide