Effects of restorative and adhesive curing methods on dentin bond strengths

Am J Dent. 2001 Jun;14(3):137-40.

Abstract

Purpose: To evaluate the shear bond strengths of "one-bottle" adhesives to dentin when used with self-cured composite.

Materials and methods: 100 bovine teeth were ground to expose superficial dentin, which was polished to 600-grit. The dentin was etched for 15 s with 35% phosphoric acid, rinsed, and blotted with tissue paper. The surface remained visibly moist for all specimens. The following adhesives were applied to the etched dentin according to manufacturers' directions: Scotchbond Multi-Purpose (in its visible light-cured [VLC] and self-cure modes) as a control, One-Step (VLC only), OptiBond Solo Plus (VLC only), Prime & Bond NT (VLC) and Prime & Bond NT Dual-Cure. For each adhesive, specimens were bonded with a self-cure composite, while 10 were bonded with a VLC composite as a control. After 24 hrs water storage, shear bond strengths were determined using an Instron universal testing machine. Data were analyzed using two-way ANOVA, Tukey's test, and Student's t-tests.

Results: Using the light-cured composite, mean bond strengths ranged from 11.0 MPa for light-cured Prime & Bond NT to 26.3 MPa for OptiBond Solo Plus. Using the self-cure composite, mean bond strengths ranged from 0.0 for light-cured Prime & Bond NT to 21.4 MPa for One-Step. Two adhesives, light-cured Prime & Bond NT and OptiBond Solo Plus, had significantly lower bond strengths when used with the self-cure composite.

Clinical significance: Some "one-bottle" dentin adhesives may not provide acceptable bonding to tooth structure when they are used with self-cure composites.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Acid Etching, Dental / methods
  • Analysis of Variance
  • Animals
  • Bisphenol A-Glycidyl Methacrylate / chemistry
  • Cattle
  • Composite Resins / chemistry*
  • Dental Bonding / methods*
  • Dental Restoration, Permanent / methods*
  • Dental Stress Analysis / instrumentation
  • Dentin / ultrastructure*
  • Dentin-Bonding Agents / chemistry*
  • Light
  • Methacrylates / chemistry
  • Phosphoric Acids / administration & dosage
  • Polymethacrylic Acids / chemistry
  • Resin Cements / chemistry
  • Statistics as Topic
  • Stress, Mechanical
  • Time Factors
  • Water

Substances

  • Bis-GMA, BPDM, HEMA dental-bonding resin
  • Composite Resins
  • Dentin-Bonding Agents
  • Methacrylates
  • OptiBond SOLO
  • Phosphoric Acids
  • Polymethacrylic Acids
  • Prime & Bond
  • Resin Cements
  • Scotchbond Multi-Purpose
  • Water
  • Bisphenol A-Glycidyl Methacrylate