Isolation and characterization of all eight bisadducts of fulleropyrrolidine derivatives

K Kordatos; S Bosi; T Da Ros; A Zambon; V Lucchini; M Prato

doi:10.1021/jo001708z

Isolation and characterization of all eight bisadducts of fulleropyrrolidine derivatives

J Org Chem. 2001 Apr 20;66(8):2802-8. doi: 10.1021/jo001708z.

Authors

K Kordatos¹, S Bosi, T Da Ros, A Zambon, V Lucchini, M Prato

Affiliation

¹ Dipartimento di Scienze Farmaceutiche, Università di Trieste, Piazzale Europa 1, 34127 Trieste, Italy.

PMID: 11304204
DOI: 10.1021/jo001708z

Abstract

We report the isolation and characterization of bisadducts of fulleropyrrolidine derivatives. The compounds were characterized by means of a variety of spectroscopic techniques, including ES-MS, UV-vis, (1)H NMR, and (13)C NMR. The whole series of bisadducts was separated for the first time in the case of the bispyrrolidines, and the determination of their structure was obtained by NMR spectroscopy with the help of HMQC and HMBC techniques.