Determination of oxalate, sulfate and nitrate in honey and honeydew by ion-chromatography

J Chromatogr A. 2000 Jun 9;881(1-2):629-38. doi: 10.1016/s0021-9673(00)00271-5.

Abstract

An ion chromatographic method for determining the anions oxalate, sulfate and nitrate in honey and honeydew samples is described. To prevent matrix interference and to isolate the anions a clean-up step using solid-phase extraction on anionic cartridges and eluting with a 0.01 M chromate solution is recommended. The anions are separated on an anionic column with a mobile phase of borate-gluconate buffer and using conductimetric detection. The method is applied to the analysis of samples from different botanical origin.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Calibration
  • Chromatography, Liquid / methods*
  • Fruit / chemistry*
  • Honey / analysis*
  • Nitrates / analysis*
  • Oxalic Acid / analysis*
  • Sensitivity and Specificity
  • Sulfates / analysis*

Substances

  • Nitrates
  • Sulfates
  • Oxalic Acid