Investment strength as a function of time and temperature

J Dent. 1999 May;27(4):297-302. doi: 10.1016/s0300-5712(98)00055-4.

Abstract

Objectives: The purpose of this investigation was to evaluate and compare the compressive strength characteristics of selected investments and to determine if these change as a function of time and temperature after mixing.

Methods: Two phosphate-bonded investments and one gypsum-bonded investment were selected and 288 cylindrical specimens were fabricated (n = 9). Baseline compressive strength values were determined for each material at room temperature and compressive strength measurements were made for all materials at 700 degrees C, and at 872 degrees C only for phosphate-bonded investments. Each material was tested at 2, 6, 12, and 24 h after mixing. Specimens were heated at 15 degrees C/min and heat soaked for 5 min in a burnout oven at the applicable testing temperature. They were transferred to a preheated chamber on an Instron testing machine and subjected to a compressive load at a crosshead speed of 2 mm/min until failure. The resulting strength data are presented in MN/m2.

Results: The gypsum-bonded investment did not exhibit marked differences in strength as a function of either time or temperature. The phosphate-bonded investments, on the other hand, demonstrated considerable changes in compressive strength and differed in compressive strength characteristics at 700 degrees C and 872 degrees C respectively.

Conclusions: At elevated temperatures, all materials approximated peak strength 2 h after initial mixing. At room temperature, the phosphate-bonded investments in this study were not significantly stronger than the gypsum-bonded investment material. However, they exhibited increased compressive strength as a function of time and temperature that was considerably higher than that exhibited by the gypsum-bonded investments.

Publication types

  • Comparative Study

MeSH terms

  • Analysis of Variance
  • Calcium Sulfate / chemistry
  • Compressive Strength
  • Dental Casting Investment / chemistry*
  • Magnesium Compounds / chemistry
  • Materials Testing / methods
  • Materials Testing / statistics & numerical data
  • Phosphates / chemistry
  • Struvite
  • Temperature
  • Time Factors

Substances

  • Dental Casting Investment
  • Magnesium Compounds
  • Phosphates
  • cerafina
  • ceramigold
  • novocast
  • Struvite
  • Calcium Sulfate