Optimization of Actuation Load and Shape Recovery Speed of Polyester-Based/Fe3O4 Composite Foams

Materials (Basel). 2021 Mar 7;14(5):1264. doi: 10.3390/ma14051264.

Abstract

In this research, polyester-based polymers/Fe3O4 nanocomposite foams were prepared in order to study their performance; namely shape recovery speed and actuation load. A foamed structure was obtained through a solid-state foaming process, which was studied and optimized in previous research. The optimum foaming parameters were applied in an attempt to achieve the highest foaming ratio possible. A Taguchi Map was then designed to determine the number of experiments to be conducted. The experimental results showed that the maximum actuation load obtained was 3.35 N, while optimal (fastest) recovery speed was 6.36 mm/min. Furthermore, temperature had no impact on the actuation load as long as a temperature above the Tg was applied. Moreover, the addition of nanoparticles reduced shape recovery speed due to discontinuity within the polymer matrix.

Keywords: actuation load; discontinuity phase; glass transition temperature; shape memory effect; shape memory polymer.