Abstract
The novel carbon based acid has been synthesized via one-step hydrothermal carbonization of furaldehyde and hydroxyethylsulfonic acid. A highly efficient procedure for the synthesis of fructone has been developed using the novel carbon based acid. The results showed that the catalyst possessed high activity for the reaction, giving a yield of over 95%. The advantages of high activity, stability, reusability and low cost for a simple synthesis procedure and wide applicability to various diols and beta-keto esters make this novel carbon based acid one of the best choices for the reaction.
Publication types
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Research Support, Non-U.S. Gov't
MeSH terms
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Acetoacetates / chemistry*
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Alcohols / chemistry
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Carbon / chemistry*
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Catalysis
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Chemistry, Organic / methods*
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Esters / chemistry
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Heterocyclic Compounds, 1-Ring / chemical synthesis*
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Heterocyclic Compounds, 1-Ring / chemistry
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Isethionic Acid / chemistry*
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Ketones / chemical synthesis*
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Ketones / chemistry
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Microscopy, Electron, Scanning
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Perfume / chemical synthesis*
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Perfume / chemistry
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Solvents / chemistry
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Spectrophotometry, Infrared
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Time Factors
Substances
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Acetoacetates
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Alcohols
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Esters
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Heterocyclic Compounds, 1-Ring
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Ketones
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Perfume
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Solvents
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Carbon
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Isethionic Acid