Experimental and Numerical Study of Viscoelastic Properties of Polymeric Interlayers Used for Laminated Glass: Determination of Material Parameters

Materials (Basel). 2019 Jul 11;12(14):2241. doi: 10.3390/ma12142241.

Abstract

An accurate material representation of polymeric interlayers in laminated glass panes has proved fundamental for a reliable prediction of their response in both static and dynamic loading regimes. This issue is addressed in the present contribution by examining the time-temperature sensitivity of the shear stiffness of two widely used interlayers made of polyvinyl butyral (TROSIFOL BG R20) and ethylene-vinyl acetate (EVALAM 80-120). To that end, an experimental program has been executed to compare the applicability of two experimental techniques, (i) dynamic torsional tests and (ii) dynamic single-lap shear tests, in providing data needed in a subsequent calibration of a suitable material model. Herein, attention is limited to the identification of material parameters of the generalized Maxwell chain model through the combination of linear regression and the Nelder-Mead method. The choice of the viscoelastic material model has also been supported experimentally. The resulting model parameters confirmed a strong material variability of both interlayers with temperature and time. While higher initial shear stiffness was observed for the polyvinyl butyral interlayer in general, the ethylene-vinyl acetate interlayer exhibited a less pronounced decay of stiffness over time and a stiffer response in long-term loading.

Keywords: dynamic shear test; dynamic torsional test; ethylene-vinyl acetate; generalized Maxwell model; laminated glass; polymer; polyvinyl butyral; rheometer.