Synthesis and characterization of laminated Si/SiC composites

J Adv Res. 2013 Jan;4(1):75-82. doi: 10.1016/j.jare.2012.01.006. Epub 2012 Feb 23.

Abstract

Laminated Si/SiC ceramics were synthesized from porous preforms of biogenous carbon impregnated with Si slurry at a temperature of 1500 °C for 2 h. Due to the capillarity infiltration with Si, both intrinsic micro- and macrostructure in the carbon preform were retained within the final ceramics. The SEM micrographs indicate that the final material exhibits a distinguished laminar structure with successive Si/SiC layers. The produced composites show weight gain of ≈5% after heat treatment in air at 1300 °C for 50 h. The produced bodies could be used as high temperature gas filters as indicated from the permeability results.

Keywords: Laminates; Microstructure; Oxidation resistance; Permeability; Si/SiC composites.