Effect of electrical discharge machining on dental Y-TZP ceramic-resin bonding

J Prosthodont Res. 2017 Apr;61(2):158-167. doi: 10.1016/j.jpor.2016.07.006. Epub 2016 Aug 27.

Abstract

Purpose: The study determined (i) the effects of electrical discharge machining (EDM) on the shear-bond strength (SBS) of the bond between luting resin and zirconia ceramic and (ii) zirconia ceramic's flexural strength with the three-point bending (TPB) test.

Methods: Sixty 4.8mm×4.8mm×3.2mm zirconia specimens were fabricated and divided into four groups (n=15): SBG: sandblasted+silane, TSCG: tribochemical silica coated+silane, LTG: Er:YAG laser treated+silane, EDMG: EDM+silane. The specimens were then bonded to a composite block with a dual-cure resin cement and thermal cycled (6000 times) prior to SBS testing. The SBS tests were performed in a universal testing machine. The SBS values were statistically analyzed using ANOVA and Tukey's test. To determine flexural strength, sixty zirconia specimens were prepared and assigned to the same groups (n=15) mentioned earlier. After surface treatment TPB tests were performed in a universal testing machine (ISO 6872). The flexural strength values were statistically analyzed using ANOVA and Tukey's test (α=0.05).

Results: The bond strengths for the four test groups (mean±SD; MPa) were as follows: SBG (Control), 12.73±3.41, TSCG, 14.99±3.14, LTG, 7.93±2.07, EDMG, 17.05±2.71. The bond strength of the EDMG was significantly higher than those of the SBG and LTG (p<0.01). The average flexural strength values for the groups SBG (Control), TSCG, LTG and EDMG were 809.47, 800.47, 679.19 and 695.71MPa, respectively (p>0.05).

Conclusions: The EDM process improved the SBS. In addition, there was no significant adverse effect of EDM on the flexural strength of zirconia.

Keywords: Bonding strength; Electrical discharge machining; Flexural strength; Graphite powder; Zirconia ceramic.

MeSH terms

  • Dental Bonding*
  • Electrochemical Techniques / methods*
  • Graphite
  • Materials Testing / methods*
  • Powders
  • Resins, Synthetic*
  • Shear Strength
  • Yttrium*
  • Zirconium*

Substances

  • Powders
  • Resins, Synthetic
  • yttria stabilized tetragonal zirconia
  • Yttrium
  • Graphite
  • Zirconium
  • zirconium oxide