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Extraction and determination of sulfonamides, macrolides, and trimethoprim in sewage sludge.
J Chromatogr A. 2005 Sep 2;1085(2):179-89. doi: 10.1016/j.chroma.2005.05.051.
J Chromatogr A. 2005.
PMID: 16106697
A mixture of water/methanol (50:50, v/v) was found as the most efficient extraction solvent. A temperature of 100 degrees C and a pressure of 100 bar were chosen for extraction. Two cycles of 5 min each efficiently extracted at least 97% of the total extractable amount of …
A mixture of water/methanol (50:50, v/v) was found as the most efficient extraction solvent. A temperature of 100 degrees C and a pre …
Utilization of large volume zwitterionic hydrophilic interaction liquid chromatography for the analysis of polar pharmaceuticals in aqueous environmental samples: Benefits and limitations.
Boulard L, Dierkes G, Ternes T.
Boulard L, et al.
J Chromatogr A. 2018 Feb 2;1535:27-43. doi: 10.1016/j.chroma.2017.12.023. Epub 2017 Dec 11.
J Chromatogr A. 2018.
PMID: 29325802
These matrix effects and those of other analytes could be efficiently compensated by using deuterated, (13)C and (15)N-labeled internal standards. The developed method was able to detect the selected 27 analytes in treated wastewater, surface water and groundwater down to …
These matrix effects and those of other analytes could be efficiently compensated by using deuterated, (13)C and (15)N-labeled intern …
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The determination of the linear alkylbenzene sulfonate isomers in water samples by gas-chromatography/mass spectrometry.
Moldovan Z, Avram V, Marincas O, Petrov P, Ternes T.
Moldovan Z, et al.
J Chromatogr A. 2011 Jan 14;1218(2):343-9. doi: 10.1016/j.chroma.2010.11.043. Epub 2010 Nov 27.
J Chromatogr A. 2011.
PMID: 21159344
This paper presents the mass spectra of 20 compounds, the proposed mechanism of formation of the diagnostic ions obtained by EI-MS and the distribution of individual isomers in water samples collected from compartments of WWTP. The individual isomers from four homolog series C …
This paper presents the mass spectra of 20 compounds, the proposed mechanism of formation of the diagnostic ions obtained by EI-MS and the d …
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