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Combining methods for speeding up multi-dimensional acquisition. Sparse sampling and fast pulsing methods for unfolded proteins.
Marion D. Marion D. J Magn Reson. 2010 Sep;206(1):81-7. doi: 10.1016/j.jmr.2010.06.007. Epub 2010 Jun 12. J Magn Reson. 2010. PMID: 20594882
We have adapted the series of 3D BEST-experiments proposed by Lescop et al. [E. Lescop, P. Schanda, B. Brutscher, A set of BEST triple-resonance experiments for time-optimized protein resonance assignment, J. ...
We have adapted the series of 3D BEST-experiments proposed by Lescop et al. [E. Lescop, P. Schanda, B. Brutscher, A set …
Impact of Intermolecular Non-Covalent Interactions in a CuI 8 PdII 1 Discrete Assembly: Conformers' Geometries and Stimuli-Sensitive Luminescence Properties.
Moutier F, Schiller J, Lecourt C, Khalil AM, Delmas V, Calvez G, Costuas K, Lescop C. Moutier F, et al. Chemistry. 2022 Apr 27;28(24):e202104497. doi: 10.1002/chem.202104497. Epub 2022 Mar 23. Chemistry. 2022. PMID: 35213070
Calculations also revealed that a more stable conformation B(calc) is expected in vacuum, which bears a different distribution of Cu(I) -Cu(I) intermetallic distances than the dications in B(o) and B(c) phases. ...Indeed, by applying mechanical or thermal str …
Calculations also revealed that a more stable conformation B(calc) is expected in vacuum, which bears a different distribution of Cu( …
Natural Chlordecone Degradation Revealed by Numerous Transformation Products Characterized in Key French West Indies Environmental Compartments.
Chevallier ML, Della-Negra O, Chaussonnerie S, Barbance A, Muselet D, Lagarde F, Darii E, Ugarte E, Lescop E, Fonknechten N, Weissenbach J, Woignier T, Gallard JF, Vuilleumier S, Imfeld G, Le Paslier D, Saaidi PL. Chevallier ML, et al. Environ Sci Technol. 2019 Jun 4;53(11):6133-6143. doi: 10.1021/acs.est.8b06305. Epub 2019 May 22. Environ Sci Technol. 2019. PMID: 31082212
In addition to previously reported, partly characterized hydrochlordecones and polychloroindenes (families A and B), we discovered 14 new chlordecone TPs, assigned to four families (B, C, D, and E). Organic synthesis and NMR analyses allowed us to achieve the comple …
In addition to previously reported, partly characterized hydrochlordecones and polychloroindenes (families A and B), we discovered 14 …
Phosphorus centers of different hybridization in phosphaalkene-substituted phospholes.
Öberg E, Orthaber A, Lescop C, Réau R, Hissler M, Ott S. Öberg E, et al. Chemistry. 2014 Jul 1;20(27):8421-32. doi: 10.1002/chem.201402406. Epub 2014 May 30. Chemistry. 2014. PMID: 24890504 Free PMC article.
Phosphole-substituted phosphaalkenes (PPAs) of the general formula Mes*P=C(CH(3))-(C(4)H(2)P(Ph))-R 5 a-c (Mes*=2,4,6-tBu(3)Ph; R=2-pyridyl (a), 2-thienyl (b), phenyl (c)) have been prepared from octa-1,7-diyne-substituted phosphaalkenes by utilizing the Fagan-Nugent route …
Phosphole-substituted phosphaalkenes (PPAs) of the general formula Mes*P=C(CH(3))-(C(4)H(2)P(Ph))-R 5 a-c (Mes*=2,4,6-tBu(3)Ph; R=2-pyridyl …
The Bacillus subtilis YkuV is a thiol:disulfide oxidoreductase revealed by its redox structures and activity.
Zhang X, Hu Y, Guo X, Lescop E, Li Y, Xia B, Jin C. Zhang X, et al. J Biol Chem. 2006 Mar 24;281(12):8296-304. doi: 10.1074/jbc.M512015200. Epub 2006 Jan 17. J Biol Chem. 2006. PMID: 16418167 Free article.
In order to elucidate the biological function, we have determined the solution structures of both the oxidized and reduced forms of B. subtilis YkuV by NMR spectroscopy and performed biochemical studies. ...
In order to elucidate the biological function, we have determined the solution structures of both the oxidized and reduced forms of B …
Self-Assembly of Reactive Linear Cu3 Building Blocks for Supramolecular Coordination Chemistry and Their Reactivity toward E(n) Ligand Complexes.
Fleischmann M, Dütsch L, Elsayed Moussa M, Balázs G, Kremer W, Lescop C, Scheer M. Fleischmann M, et al. Inorg Chem. 2016 Mar 21;55(6):2840-54. doi: 10.1021/acs.inorgchem.5b02641. Epub 2016 Mar 3. Inorg Chem. 2016. PMID: 26950219
Although reactions of 2a-c with complexes [{CpMo(CO)2}2(mu,eta(2):eta(2)-E2)] (E = P (A1), As (A2)) led to unsymmetrically substituted [Cu3(mu-X)2(mu-dpmp)2(eta(1)-L)](+) (4a-c: X = Cl-I, L = A1; 5: X = Cl, L = A2) complexes, reactions with the cyclo-P3 complex [CpMo(CO)2(eta(3)- …
Although reactions of 2a-c with complexes [{CpMo(CO)2}2(mu,eta(2):eta(2)-E2)] (E = P (A1), As (A2)) led to unsymmetrically substituted [Cu3( …
Heme orientation modulates histidine dissociation and ligand binding kinetics in the hexacoordinated human neuroglobin.
Bocahut A, Derrien V, Bernad S, Sebban P, Sacquin-Mora S, Guittet E, Lescop E. Bocahut A, et al. J Biol Inorg Chem. 2013 Jan;18(1):111-22. doi: 10.1007/s00775-012-0956-2. Epub 2012 Nov 8. J Biol Inorg Chem. 2013. PMID: 23135388 Free PMC article.
Another distinctive feature of most mammalian Ngb is their ability to form an internal disulfide bridge that increases ligand affinity. As often seen for prosthetic heme b containing proteins, human Ngb exhibits heme heterogeneity with two alternative heme orientations wit …
Another distinctive feature of most mammalian Ngb is their ability to form an internal disulfide bridge that increases ligand affinity. As o …
Aurophilicity versus mercurophilicity: impact of d10-d10 metallophilic interactions on the structure of metal-rich supramolecular assemblies.
Vreshch V, Shen W, Nohra B, Yip SK, Yam VW, Lescop C, Réau R. Vreshch V, et al. Chemistry. 2012 Jan 9;18(2):466-77. doi: 10.1002/chem.201102389. Epub 2011 Dec 6. Chemistry. 2012. PMID: 22147678
Derivative 6 is a supramolecular rectangle in which the Hg(II)-Hg(II) metal distance suggests mercurophilic interaction, whereas 6' crystallizes as two different pseudo-polymorphs 6'a,b, that is, a one-dimensional coordination polymer and one oligomer with no short Hg(II)- …
Derivative 6 is a supramolecular rectangle in which the Hg(II)-Hg(II) metal distance suggests mercurophilic interaction, whereas 6' crystall …
14 results