Thermo-Mechanical Characterization of Metal-Polymer Friction Stir Composite Joints-A Full Factorial Design of Experiments

Polymers (Basel). 2024 Feb 22;16(5):602. doi: 10.3390/polym16050602.

Abstract

With the increasing demand for lighter, more environmentally friendly, and affordable solutions in the mobility sector, designers and engineers are actively promoting the use of innovative integral dissimilar structures. In this field, friction stir-based technologies offer unique advantages compared with conventional joining technologies, such as mechanical fastening and adhesive bonding, which recently demonstrated promising results. In this study, an aluminum alloy and a glass fiber-reinforced polymer were friction stir joined in an overlap configuration. To assess the main effects, interactions, and influence of processing parameters on the mechanical strength and processing temperature of the fabricated joints, a full factorial design study with three factors and two levels was carried out. The design of experiments resulted in statistical models with excellent fit to the experimental data, enabling a thorough understanding of the influence of rotational speed, travel speed, and tool tilt angle on dissimilar metal-to-polymer friction stir composite joints. The mechanical strength of the composite joints ranged from 1708.1 ± 45.5 N to 3414.2 ± 317.1, while the processing temperature was between 203.6 ± 10.7 °C and 251.5 ± 9.7.

Keywords: composite joints; friction stir joining; full factorial design; joint morphology; mechanical strength; processing temperature.

Grants and funding

This research was funded by the European Union under the Next Generation EU, through a grant of the Portuguese Republic’s Recovery and Resilience Plan (PRR) Partnership Agreement, within the scope of the project PRODUTECH R3—“Agenda Mobilizadora da Fileira das Tecnologias de Produção para a Reindustrialização”—aiming at the mobilization of the production technologies industry toward the reindustrialization of the manufacturing industrial fabric (Project ref. nr. 60—C645808870-00000067; Total project investment: EUR 166.988.013,71; Total Grant: EUR 97.111.730,27) and an individual FCT grant with the reference 2022.11157.BD.