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Observations on the Changing Shape of the Ice Mass and the Determination of the Sublimation End Point in Freeze-Drying: An Application for Through-Vial Impedance Spectroscopy (TVIS).
Pharmaceutics. 2021 Nov 2;13(11):1835. doi: 10.3390/pharmaceutics13111835.
Pharmaceutics. 2021.
PMID: 34834255
Free PMC article.
Determination of ice interface temperature, sublimation rate and the dried product resistance, and its application in the assessment of microcollapse using through-vial impedance spectroscopy.
Jeeraruangrattana Y, Smith G, Polygalov E, Ermolina I.
Jeeraruangrattana Y, et al. Among authors: polygalov e.
Eur J Pharm Biopharm. 2020 Jul;152:144-163. doi: 10.1016/j.ejpb.2020.04.015. Epub 2020 Apr 28.
Eur J Pharm Biopharm. 2020.
PMID: 32353532
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An impedance-based process analytical technology for monitoring the lyophilisation process.
Smith G, Polygalov E, Arshad MS, Page T, Taylor J, Ermolina I.
Smith G, et al. Among authors: polygalov e.
Int J Pharm. 2013 Jun 5;449(1-2):72-83. doi: 10.1016/j.ijpharm.2013.03.060. Epub 2013 Apr 13.
Int J Pharm. 2013.
PMID: 23591008
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Through-vial impedance spectroscopy of critical events during the freezing stage of the lyophilization cycle: the example of the impact of sucrose on the crystallization of mannitol.
Arshad MS, Smith G, Polygalov E, Ermolina I.
Arshad MS, et al. Among authors: polygalov e.
Eur J Pharm Biopharm. 2014 Aug;87(3):598-605. doi: 10.1016/j.ejpb.2014.05.005. Epub 2014 May 10.
Eur J Pharm Biopharm. 2014.
PMID: 24825125
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Through-vial impedance spectroscopy of the mechanisms of annealing in the freeze-drying of maltodextrin: the impact of annealing hold time and temperature on the primary drying rate.
Smith G, Arshad MS, Polygalov E, Ermolina I.
Smith G, et al. Among authors: polygalov e.
J Pharm Sci. 2014 Jun;103(6):1799-810. doi: 10.1002/jps.23982. Epub 2014 Apr 22.
J Pharm Sci. 2014.
PMID: 24756948
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Factors affecting the use of impedance spectroscopy in the characterisation of the freezing stage of the lyophilisation process: the impact of liquid fill height in relation to electrode geometry.
Smith G, Arshad MS, Polygalov E, Ermolina I.
Smith G, et al. Among authors: polygalov e.
AAPS PharmSciTech. 2014 Apr;15(2):261-9. doi: 10.1208/s12249-013-0054-y. Epub 2013 Dec 5.
AAPS PharmSciTech. 2014.
PMID: 24306675
Free PMC article.
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An application for impedance spectroscopy in the characterisation of the glass transition during the lyophilization cycle: the example of a 10% w/v maltodextrin solution.
Smith G, Arshad MS, Polygalov E, Ermolina I.
Smith G, et al. Among authors: polygalov e.
Eur J Pharm Biopharm. 2013 Nov;85(3 Pt B):1130-40. doi: 10.1016/j.ejpb.2013.08.004. Epub 2013 Aug 16.
Eur J Pharm Biopharm. 2013.
PMID: 23959072
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