[TLC scanning determination of baicalin content in niuhuang qingxin pills]

Zhongguo Zhong Yao Za Zhi. 1995 Jan;20(1):33-4, 62.
[Article in Chinese]

Abstract

Baicalin in the samples was extracted with ultrasonic wave, the extract was spotted on thin-layer plates of gel GF254 and developed with the mobile phase consisting of toluene-ethylacetate-formic acid (2:3:2.2). Determinations were carried out with Shimadzu CS-930 TLC scanner with lambda s = 280 nm and lambda R = 207 nm. The linear range was 0.46-4.6 micrograms/ml. The average recovery of baicalin from the samples was 98.35%, RSD = 2.82%.

Publication types

  • English Abstract

MeSH terms

  • Anti-Infective Agents / analysis*
  • Chromatography, Thin Layer
  • Densitometry
  • Drug Combinations
  • Drugs, Chinese Herbal / chemistry*
  • Flavonoids / analysis*

Substances

  • Anti-Infective Agents
  • Drug Combinations
  • Drugs, Chinese Herbal
  • Flavonoids
  • niuhuang qingxin
  • baicalin