17O magic-angle spinning nuclear magnetic resonance of CaCO3

M E Smith; S Steuernagel; H J Whitfield

doi:10.1016/0926-2040(95)00010-n

17O magic-angle spinning nuclear magnetic resonance of CaCO3

Solid State Nucl Magn Reson. 1995 Jul;4(5):313-6. doi: 10.1016/0926-2040(95)00010-n.

Authors

M E Smith¹, S Steuernagel, H J Whitfield

Affiliation

¹ Physics Laboratory, University of Kent, Canterbury, UK.

PMID: 7583068
DOI: 10.1016/0926-2040(95)00010-n

Abstract

The first 17O magic-angle spinning nuclear magnetic resonance (MAS-NMR) from a carbonate ion in an inorganic compound is reported. The 17O MAS centreband of CaCO3 can be simulated with parameters CQ = 6.97 MHz, eta approximately 1 and an isotropic chemical shift of 204 ppm.

Publication types

Research Support, Non-U.S. Gov't

MeSH terms

Calcium Carbonate / chemistry*
Magnetic Resonance Spectroscopy / methods*
Oxygen Isotopes
Sensitivity and Specificity

Substances

Oxygen Isotopes
Calcium Carbonate