In situ reduction of Ag nanoparticles using okra polysaccharides for the preparation of flexible multifunctional sensors

Int J Biol Macromol. 2024 Feb;257(Pt 2):128735. doi: 10.1016/j.ijbiomac.2023.128735. Epub 2023 Dec 11.

Abstract

This paper reports the fabrication of flexible films loaded with Ag nanoparticles (Ag NPs) and annotated as POPA films from polyvinyl alcohol, okra polysaccharides, phytic acid, and AgNO3 via an in situ reduction and solution-casting method. The prepared films exhibit strain, temperature, and humidity sensing. As a flexible strain sensor, the POPA sensor has a wide strain sensing range (1-250 %), and fast response/recovery (0.22/0.28 s), while as a temperature sensor, it senses the human body temperature and exhibits excellent temperature sensitivity (TCR = -1.401 % °C-1) and good linearity (R2 = 0.994) in the temperature range of 30-55 °C. Additionally, in the relative humidity (RH) of range 35-95 %, the POPA humidity sensor outputs stable electrical signals during adsorption and desorption. Moreover, it exhibits low hysteresis values (3.19 % RH) and good linearity (R2 = 0.989) for the detection of breathing rates during different human body states. Consequently, the POPA sensor exhibits good stability, repeatability, and reversibility for strain, temperature, and humidity sensing. The designed multifunctional POPA sensor thus holds great potential for its application in flexible wearable devices and electronics.

Keywords: Humidity sensor; In situ reduction; Okra polysaccharides; Strain sensor; Temperature sensor.

MeSH terms

  • Abelmoschus*
  • Adsorption
  • Humans
  • Metal Nanoparticles*
  • Polysaccharides
  • Silver

Substances

  • Silver
  • Polysaccharides